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Perfluorocarboxylic acids (PFCAs) and perfluoroalkyl sulfonates (PFASs) in surface and tap water around Lake Taihu in China

Yong QIU, He JING, Hanchang SHI,

Frontiers of Environmental Science & Engineering 2010, Volume 4, Issue 3,   Pages 301-310 doi: 10.1007/s11783-010-0236-8

Abstract: Perfluorinated compounds (PFCs) are ubiquitously distributed in the environment mainly as perfluoro-carboxylic acids (PFCAs) and perfluoroalkyl sulfonates (PFASs). In this paper, six PFCAs and two PFASs were quantified in surface and tap water samples from 12 sites around Lake Taihu near Shanghai City in East China. Predominant PFCs were perfluorooctanoic acid (PFOA) and perfluorooctane sulfonate (PFOS), of which the concentration ranges were 6.8–206 and 1.2–45 ng·L, the geometric means were 35.3 and 9.4 ng·L, and the median (quartile range) values were 31.4 (34.4) and 10.4 (10.7) ng·L, respectively. Other PFCs were also detected but in much lower concentrations than PFOA. The sources of the PFCs were expected to be direct industrial discharges in the Lake Taihu area, and this area was also a possible source of PFCs contaminations in Shanghai district in the downstream. PFCs distributions were found different in the upstream, downstream and north part of Lake Taihu. Occurrences of PFCs in the tap water in Lake Taihu area indicated their exposure to the local people. A brief estimation of the environmental risks by PFCs implied no acute or immediate risks from PFCs to local human health, but chronic risks from PFOA in the tap water should be considered in the downstream regions.

Keywords： surface and tap water     perfluorocarboxylic acids (PFCAs)     perfluoroalkyl sulfonates (PFASs)     Lake Taihu area     ultraperformance liquid chromatography with tandem mass spectrometry (UPLC-MS)    

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Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquidchromatography–tandem mass spectrometry

WEI Yimei,ZHANG Yuan,XU Jian,GUO Changsheng,LI Lei,FAN Wenhong

Frontiers of Environmental Science & Engineering 2014, Volume 8, Issue 3,   Pages 357-371 doi: 10.1007/s11783-013-0580-6

Abstract: Sediment samples were solvent-extracted, followed by tandem SPE (strong anion exchange (SAX) + HLB) clean-upsLiquid chromatography–tandem mass spectrometry (LC-MS/MS) with multiple reaction monitoring (MRM) detection

Keywords： antibiotics     liquid chromatography–tandem mass spectrometry (LC-MS/MS)     water     sediment     fish muscle    

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Detecting

Chengkun WANG, Xiaojian ZHANG, Jun WANG, Chao CHEN

Frontiers of Environmental Science & Engineering 2012, Volume 6, Issue 6,   Pages 770-777 doi: 10.1007/s11783-012-0412-0

Abstract: An ultra-performance liquid chromatography-tandem mass spectrometry method with solid phase extractionThe solid phase extraction procedures including pH, enrichment process and MS/MS parameters including

Keywords： N-nitrosamines     water treatment plant     distribution system     ultra-performance liquid chromatography-tandem    

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An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal

Feng Zhu, Zhijian Yao, Wenliang Ji, Deye Liu, Hao Zhang, Aimin Li, Zongli Huo, Qing Zhou

Frontiers of Environmental Science & Engineering 2020, Volume 14, Issue 3, doi: 10.1007/s11783-020-1228-y

Abstract: Detection limits of method (SPE-UPLC-MS/MS) ranged between 0.03 and 0.6 ng/L. 22 PPCPs were determinedoptimal conditions, the average absolute recovery of 44 PPCPs was 75.6% using GCHM, indicating a better performanceSPE with home-made hydrophilic polymeric sorbent followed by ultra-performance liquid chromatographyand tandem mass spectrometry was validated, and the method achieved good linearity (r2>0.991, for all

Keywords： Hydrophilic resin     Solid phase extraction     Pharmaceuticals and personal care product     Ultra-performanceliquid chromatography and tandem mass spectrometry     Environmental water    

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Trace analysis of off-flavor/odor compounds in water using liquid-liquid microextraction coupled withgas chromatography—positive chemical ionization-tandem mass spectrometry

Jian LU,Paul S. WILLS,P. CHRIS WILSON

Frontiers of Environmental Science & Engineering 2016, Volume 10, Issue 3,   Pages 477-481 doi: 10.1007/s11783-015-0820-z

Abstract: friendly method was developed for analysis of off-flavor/odor compounds in fresh and salt water using gas chromatographywith chemical ionization-tandem mass spectrometry.

Keywords： off-flavor/odor compounds     liquid-liquid microextraction     gas chromatography-tandem mass spectrometry    

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Fast determination of tobramycin by reversed-phase ion-pair high performance liquid chromatography with

Liang ZHU, Jingkang WANG

Frontiers of Chemical Science and Engineering 2013, Volume 7, Issue 3,   Pages 322-328 doi: 10.1007/s11705-013-1348-z

Abstract: This method used reversed-phase ion-pair high performance liquid chromatography (HPLC) with a refractive

Keywords： tobramycin     aminoglycoside     refractive index detector     high-performance liquid chromatography     ion-pairing    

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Characteristics and removal mechanism of the precursors of N-chloro-2,2-dichloroacetamide in a drinking water treatment process at Taihu Lake

Frontiers of Environmental Science & Engineering 2021, Volume 15, Issue 5, doi: 10.1007/s11783-020-1338-6

Abstract:

• N-Cl-DCAM, an emerging N-DBP in drinking water was investigated.

Keywords： N-chloro-2     2-dichloroacetamide     Liquid chromatography with tandem mass spectrometry     Precursors     Removal    

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Application of high-speed counter-current chromatography coupled with high performance liquid chromatography

Shengguo DENG, Zeyuan DENG, Yawei FAN, Jing LI, Rong LIU, Dongmei XIONG,

Frontiers of Chemical Science and Engineering 2009, Volume 3, Issue 4,   Pages 375-382 doi: 10.1007/s11705-009-0247-9

Abstract: -β-D-glucopyranoside was separated and purified by semi-preparative high-speed counter-current chromatographyA total of 5.0mg of the targeted compound with a purity of 98.6% as determined by high performanceliquid chromatography (HPLC) was obtained from 100m g of the crude extract cleaned up by AB-flavonoid glycoside from the leaves of , and its chemical structure was identified by means of ESI-MS

Keywords： two-phase-solvent     flavonoid glycoside     high-speed counter-current     macroporous     counter-current chromatography    

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Photocatalytic degradation of methyl orange using ZnO/TiO composites

Ming GE , Changsheng GUO , Xingwang ZHU , Lili MA , Wei HU , Yuqiu WANG , Zhenan HAN ,

Frontiers of Environmental Science & Engineering 2009, Volume 3, Issue 3,   Pages 271-280 doi: 10.1007/s11783-009-0035-2

Abstract: A sample analysis was conducted using liquid chromatography coupled with electrospray ionization ion-trap

Keywords： photocatalytic degradation     methyl orange     ZnO/TiO2 composites     high performance liquid chromatographymass spectrometry (HPLC-MS)    

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Analysis of Brucella cellular fatty acids

Zhen-Xiang ZHAO MS, Hai JIANG MD, Bu-Yun CUI MS, Hong-Yan ZHAO, Dong-Ri PIAO MS, Lan-Yu LI, Su-Zhen HAOMS,

Frontiers of Medicine 2010, Volume 4, Issue 2,   Pages 216-219 doi: 10.1007/s11684-010-0037-2

Abstract: were harvested, saponificated, methylated and extracted to provide fatty acid methylesters for gas chromatography

Keywords： Brucella     gas chromatography     cellular fatty acids     dendrogram     typing    

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Simultaneous analysis of five taste and odor compounds in surface water using solid-phase extraction and gas chromatography-mass

Wenfeng SUN, Ruibao JIA, Baoyu GAO

Frontiers of Environmental Science & Engineering 2012, Volume 6, Issue 1,   Pages 66-74 doi: 10.1007/s11783-010-0257-3

Abstract: In this paper, a method using solid-phase extraction (SPE) and gas chromatography-mass spectrometry (GC-MS) was developed to simultaneously analyze five taste and odor compounds in surface water, i.e.,

Keywords： solid-phase extraction (SPE)     gas chromatography-mass spectrometry (GC-MS)     taste and odor compounds     surface    

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Gas marbles: ultra-long-lasting and ultra-robust bubbles formed by particle stabilization

Frontiers of Chemical Science and Engineering   Pages 1681-1687 doi: 10.1007/s11705-022-2180-0

Abstract: Their rupture can be attributed to liquid evaporation, thin film drainage and the nuclei of environmentalInspired by particle-stabilized interfaces in Pickering emulsions, armored bubbles and liquid marble,bubbles are protected by an enclosed particle-entrapping liquid thin film, and the resultant soft objectsubjected to overpressure and underpressure, owing to the compact particle monolayer straddling the surface liquid

Keywords： bubble     particles     interfaces     armored bubble     liquid marble     gas marble     Pickering emulsion    

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Performance of steel bridge deck pavement structure with ultra high performance concrete based on resin

Frontiers of Structural and Civil Engineering 2021, Volume 15, Issue 4,   Pages 895-904 doi: 10.1007/s11709-021-0759-z

Abstract: This research investigated a pavement system on steel bridge decks that use epoxy resin (EP) bonded ultra-highperformance concrete (UHPC).the interface of the pavement layer, reinforcement, and different paving materials on the structural performancea fixed force of 9 kN and a dynamic deflection of 0.35 mm, which meets the requirements for fatigue performance

Keywords： steel bridge deck pavement     ultra-high-performance concrete     epoxy resin     composite structure     bendingfatigue performance    

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Effects of fatty acid chain length and degree of unsaturation on the surface activities of monoacyl trehaloses

Yue-E SUN, Wenshui XIA, Xueyan TANG, Zhiyong HE, Jie CHEN,

Frontiers of Chemical Science and Engineering 2009, Volume 3, Issue 4,   Pages 407-412 doi: 10.1007/s11705-009-0255-9

Abstract: Monoacyl trehaloses were enzymatically synthesized and purified with silica gel column chromatographyand semi-preparative high-performance liquid chromatography (HPLC), and the purity of products was identifiedby mass spectrometry (MS) and nuclear magnetic resonance (NMR).

Keywords： high-performance liquid     tension     different     spectrometry     chromatography    

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Shear behavior of ultra-high-performance concrete beams prestressed with external carbon fiber-reinforced

Frontiers of Structural and Civil Engineering 2021, Volume 15, Issue 6,   Pages 1426-1440 doi: 10.1007/s11709-021-0783-z

Abstract: The ultra-high-performance concrete (UHPC) and fiber-reinforced polymer (FRP) are well-accepted high-performanceThe combination of these advanced materials could contribute to improvement of structural performance

Keywords： beam     external prestressing     ultra-high-performance concrete     fiber-reinforced polymers     shear behavior    

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Title Author Date Type Operation

Perfluorocarboxylic acids (PFCAs) and perfluoroalkyl sulfonates (PFASs) in surface and tap water around Lake Taihu in China

Yong QIU, He JING, Hanchang SHI,

Journal Article

Simultaneous quantification of several classes of antibiotics in water, sediments, and fish muscles by liquidchromatography–tandem mass spectrometry

WEI Yimei,ZHANG Yuan,XU Jian,GUO Changsheng,LI Lei,FAN Wenhong

Journal Article

Detecting

Chengkun WANG, Xiaojian ZHANG, Jun WANG, Chao CHEN

Journal Article

An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal

Feng Zhu, Zhijian Yao, Wenliang Ji, Deye Liu, Hao Zhang, Aimin Li, Zongli Huo, Qing Zhou

Journal Article

Trace analysis of off-flavor/odor compounds in water using liquid-liquid microextraction coupled withgas chromatography—positive chemical ionization-tandem mass spectrometry

Jian LU,Paul S. WILLS,P. CHRIS WILSON

Journal Article

Fast determination of tobramycin by reversed-phase ion-pair high performance liquid chromatography with

Liang ZHU, Jingkang WANG

Journal Article

Characteristics and removal mechanism of the precursors of N-chloro-2,2-dichloroacetamide in a drinking water treatment process at Taihu Lake

Journal Article

Application of high-speed counter-current chromatography coupled with high performance liquid chromatography

Shengguo DENG, Zeyuan DENG, Yawei FAN, Jing LI, Rong LIU, Dongmei XIONG,

Journal Article

Photocatalytic degradation of methyl orange using ZnO/TiO composites

Ming GE , Changsheng GUO , Xingwang ZHU , Lili MA , Wei HU , Yuqiu WANG , Zhenan HAN ,

Journal Article

Analysis of Brucella cellular fatty acids

Zhen-Xiang ZHAO MS, Hai JIANG MD, Bu-Yun CUI MS, Hong-Yan ZHAO, Dong-Ri PIAO MS, Lan-Yu LI, Su-Zhen HAOMS,

Journal Article

Simultaneous analysis of five taste and odor compounds in surface water using solid-phase extraction and gas chromatography-mass

Wenfeng SUN, Ruibao JIA, Baoyu GAO

Journal Article

Gas marbles: ultra-long-lasting and ultra-robust bubbles formed by particle stabilization

Journal Article

Performance of steel bridge deck pavement structure with ultra high performance concrete based on resin

Journal Article

Effects of fatty acid chain length and degree of unsaturation on the surface activities of monoacyl trehaloses

Yue-E SUN, Wenshui XIA, Xueyan TANG, Zhiyong HE, Jie CHEN,

Journal Article

Shear behavior of ultra-high-performance concrete beams prestressed with external carbon fiber-reinforced

Journal Article